Adelaide Research & Scholarship
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https://hdl.handle.net/2440/61874
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| Type: | Journal article |
| Title: | 5-Bromospiro[1,2-dioxane-4,4'-tricyclo[4.3.1.13,8]undecane]-3'-ol |
| Author: | Robinson, A. Taylor, D. Tiekink, E. |
| Citation: | Acta Crystallographica Section E: Structure Reports Online, 2010; 66(1):O247-U3231 |
| Publisher: | Blackwell Munksgaard |
| Issue Date: | 2010 |
| ISSN: | 1600-5368 1600-5368 |
| Statement of Responsibility: | T. V. Robinson, D. K. Taylor and E. R. T. Tiekink |
| Abstract: | The title compound, C14H21BrO3, comprises a seven- (C7) and three six-membered (1 × O2C4 and 2 × C6) rings, and each adopts a conformation based on a chair. Stability to the molecular structure is afforded by an intramolecular O-HBr hydrogen bond. In the crystal structure, molecules are arranged into a helical supramolecular chain along the b axis, linked by C-HO interactions, where the O-atom acceptor is one of the dioxane O atoms. The crystal studied was found to be a racemic twin. The major component was present 94% of the time. |
| Rights: | Copyright © 2010 International Union of Crystallography |
| DOI: | 10.1107/S1600536809054762 |
| Grant ID: | ARC |
| Published version: | http://dx.doi.org/10.1107/s1600536809054762 |
| Appears in Collections: | Aurora harvest 5 Chemistry publications |
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