Please use this identifier to cite or link to this item:
https://hdl.handle.net/2440/86637
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Full metadata record
DC Field | Value | Language |
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dc.contributor.author | Becker, A.M. | - |
dc.contributor.author | Irvine, R.W. | - |
dc.contributor.author | McCormick, A.S. | - |
dc.contributor.author | Russell, R.A. | - |
dc.contributor.author | Warrener, R.N. | - |
dc.date.issued | 1986 | - |
dc.identifier.citation | Tetrahedron Letters: the international journal for the rapid publication of all preliminary communications in organic chemistry, 1986; 27(29):3431-3434 | - |
dc.identifier.issn | 0040-4039 | - |
dc.identifier.issn | 1873-3581 | - |
dc.identifier.uri | http://hdl.handle.net/2440/86637 | - |
dc.description.abstract | Lithiation (n-BuLi) of the (3′-methoxyphenyl) oxazoline (2a) occurs specifically at C2′ and, following carboxylation (CO2/13CO2) and esterification, yields the phthalate derivative (e.g.5a). Elaboration of the oxazoline-ring furnishes the related aldehydes which spontaneously cyclise to form the 3-hydroxyphthalides (8/10). The title[5-13C] anthracyclinone (20) is produced from 3-cyanophthalide (11) in good yield and with excellent isotopic efficiency. | - |
dc.description.statementofresponsibility | Anna M. Becker, Robert W. Irvine, Alison S. McCormick, Richard A. Russell, Ronald N. Warrener | - |
dc.language.iso | en | - |
dc.publisher | Pergamon Press | - |
dc.rights | Copyright status unknown | - |
dc.source.uri | http://dx.doi.org/10.1016/s0040-4039(00)84815-7 | - |
dc.title | A new route to 3-hydroxyphthalides: application to the synthesis of racemic [5-¹³C] daunomycinone | - |
dc.title.alternative | A new route to 3-hydroxyphthalides: application to the synthesis of racemic [5-(13)C] daunomycinone | - |
dc.type | Journal article | - |
dc.identifier.doi | 10.1016/S0040-4039(00)84815-7 | - |
pubs.publication-status | Published | - |
Appears in Collections: | Aurora harvest 2 Chemistry publications |
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